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Modern X-ray Structure Determination (MXD)5 ECTS (englische Bezeichnung: Modern X-ray Structure Determination)
Modulverantwortliche/r: Frank Wilhelm Heinemann Lehrende:
Frank Wilhelm Heinemann
Startsemester: |
SS 2021 | Dauer: |
1 Semester | Turnus: |
halbjährlich (WS+SS) |
Präsenzzeit: |
45 Std. | Eigenstudium: |
105 Std. | Sprache: |
Englisch |
Lehrveranstaltungen:
Inhalt:
- Fundamentals of crystallization and polymorphism
Structural description of single crystals, crystal systems, unit cell, symmetry and symmetry elements, space groups
Diffraction power of crystals, diffraction conditions, structure factor
Generation of X-rays, single crystal diffractometers, detection techniques
Structure solution techniques and refinement procedures, software, problems and pitfalls, interpretation of results
Anomalous dispersion and absolute structure
Graphical representations, use of data bases
Lernziele und Kompetenzen:
Students ...
get insight into thermodynamics of crystallization and crystallization techniques
get fundamentals of the theory behind crystal structure determination
get practice in crystal selection, mounting and measurement set-up
get hands-on training in structure solution and refinement using up-to-date software
are enabled to interpret and compare results of a single crystal structure determination
Literatur:
- Werner Massa: Kristallstrukturbestimmung. Teubner Studienbücher Chemie, Vieweg und Teubner, 6. Auflage, 2009, ISBN: 3834806498
William Clegg: Crystal Structure Determination. Oxford Chemistry Primers. Oxford University Press, 1998, ISBN: 0198559011
Further literature will be recommended in the course
Bemerkung:
Module campatibility:
Organisatorisches:
- Module can be taken in winter or in summer term
Module will be taught in presence and/or online
Students have to register for the module examination (check registration periods)
Information/registration available on studon XXXXXXX
Verwendbarkeit des Moduls / Einpassung in den Musterstudienplan: Das Modul ist im Kontext der folgenden Studienfächer/Vertiefungsrichtungen verwendbar:
- Chemistry (Master of Science)
(Po-Vers. 2020w | NatFak | Chemistry (Master of Science) | Wahlmodule | Modern X-ray Structure Determination)
- Molecular Science (Master of Science): 3. Semester
(Po-Vers. 2020w | NatFak | Molecular Science (Master of Science) | Elective modules | Modern X-ray Structure Determination)
Studien-/Prüfungsleistungen:
Modern X-ray Structure Determination (Prüfungsnummer: 65581)
- Prüfungsleistung, mündliche Prüfung, Dauer (in Minuten): 20, benotet, 5 ECTS
- Anteil an der Berechnung der Modulnote: 100.0 %
- weitere Erläuterungen:
Lab report in manuscript style (max. 2000 words plus raw data); module is ungraded, but has to be passed!
- Prüfungssprache: Englisch
- Erstablegung: SS 2021
1. Prüfer: | Frank Wilhelm Heinemann |
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